1-(4-甲氧基-联苯-4-基)-乙酮合成路线 （共 91 条）
反应条件
morpholine; sodium hydroxide; sulfur 1.) reflux, 14 h, 2.) reflux, 12 h; Yield given. Multistep reaction;
参考文献
Vargha et al.
Acta Chimica Academiae Scientiarum Hungaricae, 1955 , vol. 5, p. 111,114
反应条件
1: 95 percent / NaOBr 2: 89 percent / diborane 3: 85 percent / Pb(OAc)4/Py View Scheme
参考文献
Analytical Chemistry, , vol. 52, # 14 p. 2417 - 2420
反应条件
1: Br2, KOH / dioxane 2: 80 percent / HNO3, AcOH 3: HBr, AcOH View Scheme
参考文献
Svensson, Magnus; Helgee, Bertil; Skarp, Kent; Andersson, Gunnar
Journal of Materials Chemistry, 1998 , vol. 8, # 2 p. 353 - 362
反应条件
1: 95 percent / NaOBr 2: 89 percent / diborane View Scheme
参考文献
Janini, G. M.; Sato, R. I.; Muschik, G. M.
Analytical Chemistry, 1980 , vol. 52, # 14 p. 2417 - 2420
反应条件
1: Br2, KOH / dioxane 2: HBr, AcOH View Scheme
参考文献
Svensson, Magnus; Helgee, Bertil; Skarp, Kent; Andersson, Gunnar
Journal of Materials Chemistry, 1998 , vol. 8, # 2 p. 353 - 362
反应条件
sodium hydroxide; bromine in 1,4-dioxane; water T=0°C; 3 h;
参考文献
Boehringer Ingelheim International GmbH
Patent: US2004/242572 A1, 2004 ;
Location in patent: Page/Page column 57 ;
反应条件
hydrogenchloride; bromine in water
参考文献
Societe d'Expansion Scientifique Expansia
Patent: US6160157 A1, 2000 ;
反应条件
sodium salt of phosphorous acid; palladium on activated charcoal in water; isopropyl alcohol
T=20°C; Suzuki-Miyaura coupling reaction; 48 h;
参考文献
Maegawa, Tomohiro; Kitamura, Yoshiaki; Sako, Satoko; Udzu, Takahiro; Sakurai, Ai; Tanaka, Asami; Kobayashi, Yusuke; Endo, Koichi; Bora, Utpal; Kurita, Takanori; Kozaki, Atsushi; Monguchi, Yasunari; Sajiki, Hironao
Chemistry - A European Journal, 2007 , vol. 13, # 20 p. 5937 - 5943
反应条件
aluminium trichloride in dichloromethane
1 h; Heating;
参考文献
Chan, L. K. M.; Gray, G. W.; Lacey, D.; Scrowston, R. M.; Shenouda, I. G.; Toyne, K. J.
Molecular Crystals and Liquid Crystals (1969-1991), 1989 , vol. 172, p. 125 - 146
反应条件
potassium phosphate; tetrabutylammomium bromide; chitosan-supported Pd(0) linked with diglycidyl ether PEG in water
T=150°C; Suzuki cross-coupling reaction; 0.166667 h; microwave irradiation;
参考文献
Yi, Song-Se; Lee, Dong-Ho; Sin, Eunyoung; Lee, Yoon-Sik
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6771 - 6775
