1-(4-甲氧基-联苯-4-基)-乙酮合成路线 (共 91 条)
反应条件
lithium niobate; palladium diacetate; potassium carbonate in ethanol; water; paraffin oil
T=87 - 88°C; Suzuki Coupling; 0.25 h;
参考文献
Kulkarni, Ketav; Friend, James; Yeo, Leslie; Perlmutter, Patrick
Ultrasonics Sonochemistry, 2014 , vol. 21, # 4 p. 1305 - 1309
反应条件
sodium salt of phosphorous acid; palladium on activated charcoal in water; isopropyl alcohol
T=20°C; Suzuki-Miyaura reaction; 2 h;
参考文献
Zhang, Guolin
Journal of Chemical Research, 2004 , # 9 p. 593 - 595
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; copper(l) iodide; triphenylphosphine in water; N,N-dimethyl-formamide
T=100°C; Suzuki-Miyaura cross-coupling; Inert atmosphere;
参考文献
Bonin, Helne; Leuma-Yona, Rodrigue; Marchiori, Bruno; Demonchaux, Patrice; Gras, Emmanuel
Tetrahedron Letters, 2011 , vol. 52, # 10 p. 1132 - 1135
反应条件
hydrogenchloride; acetic anhydride; aluminium chloride in ethanol; 1,2-dichloro-ethane
参考文献
Societe d'Expansion Scientifique Expansia
Patent: US6160157 A1, 2000 ;
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in water
T=80°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Zhou, Xia-Xia; Shao, Li-Xiong
Synthesis, 2011 , # 19 art. no. H53711SS, p. 3138 - 3142
反应条件
bis(η3-allyl-μ-chloropalladium(II)); triphenyl-arsane; caesium carbonate in toluene
T=90°C; 3 h;
参考文献
Denmark, Scott E.; Ober, Michael H.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1703 - 1714
反应条件
Cyphos® IL 101; potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene
T=50°C; Suzuki cross-coupling; 1 h;
参考文献
Cano, Rafael; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 2011 , vol. 67, # 30 p. 5432 - 5436
反应条件
NHC-Pd(II)-Im; tetrabutyl ammonium fluoride in toluene
T=120°C; Hiyama reaction; 3 h; Inert atmosphere;
参考文献
Gu, Zheng-Song; Shao, Li-Xiong; Lu, Jian-Mei
Journal of Organometallic Chemistry, 2012 , vol. 700, p. 132 - 134
反应条件
sodium hydroxide; dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane
T=80°C; 4 h;
参考文献
Murata; Shimazaki; Watanabe; Masuda
Synthesis, 2001 , # 15 p. 2231 - 2233
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Jadhav, Deepak N.
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6644 - 6647