1-(4-甲氧基-联苯-4-基)-乙酮合成路线 （共 91 条）
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
反应条件
morpholine; potassium phosphate; palladium diacetate in isopropyl alcohol
T=80°C; Suzuki-Miyaura Coupling; 2 h; Inert atmosphere;
参考文献
Abe, Taichi; Mino, Takashi; Watanabe, Kohei; Yagishita, Fumitoshi; Sakamoto, Masami
European Journal of Organic Chemistry, 2014 , vol. 2014, # 18 p. 3909 - 3916
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide
T=80°C; 18 h;
参考文献
Zhu, Lei; Duquette, Jason; Zhang, Mingbao
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3729 - 3732
反应条件
tri-tert-butyl phosphine; boron trifluoride diethyl etherate; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether; hexane
T=20°C; 1 h;
参考文献
Saeki, Tomoyuki; Son, Eun-Cheol; Tamao, Kohei
Organic Letters, 2004 , vol. 6, # 4 p. 617 - 619
反应条件
1: p-anisylgermanium trichloride With ammonium hydroxide
T=20°C; 1 h;
2: para-bromoacetophenone With sodium hydroxide; palladium diacetate in 1,4-dioxane; water
1 h; Heating; Further stages.;
参考文献
Endo, Mayuko; Fugami, Keigo; Enokido, Tatsuki; Sano, Hiroshi; Kosugi, Masanori
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1025 - 1027
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol
T=100°C; Suzuki-Miyaura reaction; 2 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; potassium carbonate in dimethyl sulfoxide
T=65°C; Hiyama coupling;
参考文献
Shirbin, Steven J.; Boughton, Berin A.; Zammit, Steven C.; Zanatta, Shannon D.; Marcuccio, Sebastian M.; Hutton, Craig A.; Williams, Spencer J.
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2971 - 2974
反应条件
1: 1-bromo-4-methoxy-benzene With indium; bathophenanthroline; 3-chloroprop-1-ene; lithium chloride; cobalt(II) dibromide in tetrahydrofuran
T=100°C; 23 h; Inert atmosphere;
2: 4'-iodoacetophenone With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in tetrahydrofuran
T=80°C; 17 h; Inert atmosphere;
参考文献
Adak, Laksmikanta; Yoshikai, Naohiko
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7563 - 7568
反应条件
[Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium carbonate in N,N-dimethyl-formamide
T=100°C; Stille coupling; 0.166667 h; Microwave irradiation;
参考文献
Hajipour, Abdol R.; Karami, Kazem; Rafiee, Fatemeh
Applied Organometallic Chemistry, 2012 , vol. 26, # 1 p. 27 - 31
反应条件
alginate/gellan gum beads containing Pd nanoparticles in water
T=40°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Cacchi, Sandro; Caponetti, Eugenio; Casadei, Maria Antonietta; Di Giulio, Andrea; Fabrizi, Giancarlo; Forte, Giovanni; Goggiamani, Antonella; Moreno, Sandra; Paolicelli, Patrizia; Petrucci, Francesco; Prastaro, Alessandro; Saladino, Maria Luisa
Green Chemistry, 2012 , vol. 14, # 2 p. 317 - 320
