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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
130260-02-5
合成路线
（共 6 条）
130260-00-3
→
反应条件
130260-02-5
反应条件
sulfuric acid in diethyl ether T=40 - 70°C; 3 h;
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Matousova, Oluse; Metysova, Jirina; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, p. 1297 - 1310
6789-94-2
3-氨基-N-乙基哌啶
→
反应条件
130260-02-5
反应条件
1: 81 percent / CHCl3 / 1.5 h / Heating 2: 82 percent / N2H4*H2O, Raney Ni / ethanol / 1.5 h / 60 °C 3: 94 percent / NaHCO3 / CH2Cl2 4: 67 percent / tetrabutylamonium hydrogen sulfate, KOH / CH2Cl2; H2O / 1 h / Ambient temperature 5: 83 percent / 90percent H2SO4 / diethyl ether / 3 h / 40 - 70 °C View Scheme
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Matousova, Oluse; Metysova, Jirina; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, p. 1297 - 1310
90763-46-5
→
反应条件
130260-02-5
反应条件
1: 81 percent / CHCl3 / 1.5 h / Heating 2: 82 percent / N2H4*H2O, Raney Ni / ethanol / 1.5 h / 60 °C 3: 94 percent / NaHCO3 / CH2Cl2 4: 67 percent / tetrabutylamonium hydrogen sulfate, KOH / CH2Cl2; H2O / 1 h / Ambient temperature 5: 83 percent / 90percent H2SO4 / diethyl ether / 3 h / 40 - 70 °C View Scheme
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Matousova, Oluse; Metysova, Jirina; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, p. 1297 - 1310
130259-96-0
→
反应条件
130260-02-5
反应条件
1: 67 percent / tetrabutylamonium hydrogen sulfate, KOH / CH2Cl2; H2O / 1 h / Ambient temperature 2: 83 percent / 90percent H2SO4 / diethyl ether / 3 h / 40 - 70 °C View Scheme
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Matousova, Oluse; Metysova, Jirina; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, p. 1297 - 1310
130259-92-6
→
反应条件
130260-02-5
反应条件
1: 94 percent / NaHCO3 / CH2Cl2 2: 67 percent / tetrabutylamonium hydrogen sulfate, KOH / CH2Cl2; H2O / 1 h / Ambient temperature 3: 83 percent / 90percent H2SO4 / diethyl ether / 3 h / 40 - 70 °C View Scheme
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Matousova, Oluse; Metysova, Jirina; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, p. 1297 - 1310
4840-67-9
→
反应条件
130260-02-5
反应条件
1: 82 percent / N2H4*H2O, Raney Ni / ethanol / 1.5 h / 60 °C 2: 94 percent / NaHCO3 / CH2Cl2 3: 67 percent / tetrabutylamonium hydrogen sulfate, KOH / CH2Cl2; H2O / 1 h / Ambient temperature 4: 83 percent / 90percent H2SO4 / diethyl ether / 3 h / 40 - 70 °C View Scheme
参考文献
Valenta, Vladimir; Holubek, Jiri; Svatek, Emil; Matousova, Oluse; Metysova, Jirina; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, p. 1297 - 1310
