1: 89 percent / tetrahydrofuran / 1 h / 0 °C 2: 98 percent / LiCl, NaBH4 / ethanol / 17 h / Ambient temperature 3: 81 percent / SO3*Py, Et3N / toluene; dimethylsulfoxide / 0.33 h / Ambient temperature 4: 100 percent / benzyltributylammonium chloride / CH2Cl2; H2O / 3 h / 0 °C 5: 100 percent / aq. HCl / ethyl acetate / 14 h / 80 - 100 °C View Scheme
参考文献
Matsuda, Fuyuhiko; Mtsumoto, Teruyo; Ohsaki, Masako; Ito, Yoshio; Terashima, Shiro
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 2 p. 360 - 365
1: 89 percent / tetrahydrofuran / 1 h / 0 °C 2: 98 percent / LiCl, NaBH4 / ethanol / 17 h / Ambient temperature 3: 81 percent / SO3*Py, Et3N / toluene; dimethylsulfoxide / 0.33 h / Ambient temperature 4: 100 percent / benzyltributylammonium chloride / CH2Cl2; H2O / 3 h / 0 °C 5: 50 percent / aq. HCl / ethyl acetate / 14 h / 80 - 100 °C View Scheme
参考文献
Matsuda, Fuyuhiko; Mtsumoto, Teruyo; Ohsaki, Masako; Ito, Yoshio; Terashima, Shiro
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 2 p. 360 - 365
