反应条件
1: toluene / 5.5 h / |Inert atmosphere; |Reflux 2: toluene / 14.08 h / 0 - 20 °C / |Inert atmosphere 3: potassium hydrogensulfate; water / tert-butyl methyl ether / 4 h / 20 °C / |Inert atmosphere 4: magnesium sulfate; sodium tetrahydroborate / ethanol / 22 h / 20 - 70 °C / |Inert atmosphere View Scheme
参考文献
Seifert, Katrin; Buettner, Anita; Rigol, Stephan; Eilert, Nicole; Giannis, Athanassios; Wandel, Elke
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 21 p. 6465 - 6481,17