β-D-呋喃核糖-1,2,3,5-四乙酸酯合成路线 （共 86 条）
参考文献
Helvetica Chimica Acta, , vol. 37, p. 1373,1375
Chemische Berichte, , vol. 83, p. 153
Chemische Berichte, , vol. 86, p. 817,822
参考文献
Chemische Berichte, , vol. 83, p. 153
Chemische Berichte, , vol. 86, p. 817,822
反应条件
ammonium sulfate; chloro-trimethyl-silane; tin(IV) chloride 1.) hexachlorotrimethyldisilazane, reflux, 16 h, 2.) dichloroethane, r.t., 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hasan; Lambert; Srivastava
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 1877 - 1883
反应条件
1: 95 percent / CF3SO3SiMe3 / acetonitrile / reflux, 1h; rt, 16 h 2: 1,8-diazabicyclo<5.4.0>undec-7-ene / acetonitrile 3: hydrogen / Pd/C / 16 h / 3102.9 Torr / Ambient temperature View Scheme
参考文献
Raju, Natarajan; Robins, Roland K.; Vaghefi, Morteza M.
Journal of the Chemical Society, Chemical Communications, 1989 , # 2 p. 1769 - 1770
反应条件
1: trifluorormethanesulfonic acid / 2 h / 135 °C / 55 Torr 2: ammonia / methanol / 40 h / 20 °C View Scheme
参考文献
Li; Zhang; Mei; Tan
Organic Preparations and Procedures International, 2012 , vol. 44, # 4 p. 387 - 391
反应条件
1: 1 h / 170 - 180 °C / 20 Torr 2: NaOMe / methanol View Scheme
参考文献
Ruf, Klaus; Pfleiderer, Wolfgang
Carbohydrate Research, 1991 , vol. 216, # 1 p. 421 - 439
反应条件
trimethylsilyl trifluoromethanesulfonate; 1,1,1,3,3,3-hexamethyl-disilazane; 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide in acetonitrile Vorbrueggen Nucleoside Synthesis; Microwave irradiation;
参考文献
Parmenopoulou, Vanessa; Chatzileontiadou, Demetra S.M.; Manta, Stella; Bougiatioti, Stamatina; Maragozidis, Panagiotis; Gkaragkouni, Dimitra-Niki; Kaffesaki, Eleni; Kantsadi, Anastassia L.; Skamnaki, Vassiliki T.; Zographos, Spyridon E.; Zounpoulakis, Panagiotis; Balatsos, Nikolaos A.A.; Komiotis, Dimitris; Leonidas, Demetres D.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 24 p. 7184 - 7193
反应条件
BiBr3; trimethylsilyl bromide 1) CH2Cl2, rt, 10 min; 2) CH3CN, rt, 4 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Winum, Jean-Yves; Kamal, Mehrnaz; Barragan, Veronique; Leydet, Alain; Montero, Jean-Louis
Synthetic Communications, 1998 , vol. 28, # 4 p. 603 - 606
反应条件
tin(IV) chloride in acetonitrile T=20°C;
参考文献
Hong, Wei; Dowden, James
Chinese Chemical Letters, 2011 , vol. 22, # 12 p. 1439 - 1442
反应条件
T=125°C; P=35 - 45 Torr; 3 h;
参考文献
Schmidt, Richard R.; Loesch, Gabriele R.; Fischer, Peter
Chemische Berichte, 1980 , vol. 113, # 9 p. 2891 - 2915
