乙酸-8-壬烯-1-基酯合成路线 （共 14 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; 3,3',5,5'-tetra-tert-butyl-2,2'-di-hydroxy-1,1'-biphenyl; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in neat (no solvent) T=132°C; 3 h; Inert atmosphere;
参考文献
Liu, Yiyang; Kim, Kelly E.; Herbert, Myles B.; Fedorov, Alexey; Grubbs, Robert H.; Stoltz, Brian M.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 130 - 136
反应条件
lithium carbonate; lithium bromide in N,N-dimethyl-formamide T=120°C; 6 h;
参考文献
Huang; Li; Lu; Aisa
Chemistry of Natural Compounds, 2006 , vol. 42, # 6 p. 727 - 729
反应条件
pyridine T=20°C; 72 h;
参考文献
Mori, Kenji
Tetrahedron, 2009 , vol. 65, # 19 p. 3900 - 3909
反应条件
1: diethyl ether 2: 565 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 81, p. 4737,4741
反应条件
1: LiAlH4 / diethyl ether 2: Py / benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 14, p. 236 - 239
反应条件
ethene; [2-(1-methylethoxy-κO)phenylmethyl-κC](nitrato-κO,κO′){rel-(2R,5R,7S)-tricyclo[3.3.1.13,7]decane-2,1-diyl[3-(2,4,6-trimethylphenyl)-1-imidazolidinyl-2-ylidene]}ruthenium in tetrahydrofuran T=35°C; 4.5 h; Sealed tube;
参考文献
Miyazaki, Hiroshi; Herbert, Myles B.; Liu, Peng; Dong, Xiaofei; Xu, Xiufang; Keitz, Benjamin K.; Ung, Thay; Mkrtumyan, Garik; Houk; Grubbs, Robert H.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5848 - 5858
参考文献
Journal of the American Chemical Society, , vol. 81, p. 4737,4741
参考文献
Journal of Medicinal Chemistry, , vol. 14, p. 236 - 239
反应条件
1: 93 percent / pyridine / 24 h / 20 °C 2: 78 percent / Br2; HgO / CCl4 / 4 h / Irradiation 3: 81 percent / LiBr; Li2CO3 / dimethylformamide / 6 h / 120 °C View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 42, # 6 p. 727 - 729
反应条件
C32H41N3O4Ru in tetrahydrofuran T=20°C; 4 h; Inert atmosphereGlovebox; chemoselective reaction;
参考文献
Herbert, Myles B.; Marx, Vanessa M.; Pederson, Richard L.; Grubbs, Robert H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 1 p. 310 - 314
Angew. Chem., 2012 , vol. 125, # 1 p. 328 - 332,5
