乙酸-8-壬烯-1-基酯合成路线 (共 14 条)
反应条件
C29H36N3O4Ru in tetrahydrofuran
T=35°C; 2 h; Inert atmosphere;
参考文献
Keitz, Benjamin K.; Endo, Koji; Patel, Paresma R.; Herbert, Myles B.; Grubbs, Robert H.
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 693 - 699
反应条件
C32H43N3O4Ru in tetrahydrofuran
T=35°C; Overall yield = 67 percent;
参考文献
GRUBBS, ROBERT H.; HERBERT, MYLES B.; WICKENS, ZACHARY K.; MARX, VANESSA M.
Patent: US2013/231499 A1, 2013 ;
Location in patent: Paragraph 0215; 0217 ;
反应条件
[2-(1-methylethoxy-κO)phenylmethyl-κC](nitrato-κO,κO′){rel-(2R,5R,7S)-tricyclo[3.3.1.13,7]decane-2,1-diyl[3-(2,4,6-trimethylphenyl)-1-imidazolidinyl-2-ylidene]}ruthenium in tetrahydrofuran
T=35°C; 6 h; GloveboxInert atmosphere;
参考文献
Miyazaki, Hiroshi; Herbert, Myles B.; Liu, Peng; Dong, Xiaofei; Xu, Xiufang; Keitz, Benjamin K.; Ung, Thay; Mkrtumyan, Garik; Houk; Grubbs, Robert H.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5848 - 5858
反应条件
(pivalate)(o-isopropoxyphenylmethylene)(1,3-di(2,4,6-trimethylphenyl)imidazolidin-2-yl-H)ruthenium in tetrahydrofuran
T=35°C; 2 h; GloveboxInert atmosphere;
参考文献
Miyazaki, Hiroshi; Herbert, Myles B.; Liu, Peng; Dong, Xiaofei; Xu, Xiufang; Keitz, Benjamin K.; Ung, Thay; Mkrtumyan, Garik; Houk; Grubbs, Robert H.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5848 - 5858