in neat (no solvent) on heating;; product-mixture;;
参考文献
Duval, C.
Microchimica Acta, 1956 , p. 1432 - 1432
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Gmelin Handbook: Na: SVol.2, 98, page 820 - 822
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反应条件
in neat (no solvent) byproducts: SO3; prepn. by flow method; Bi2O3, Fe2O3 placed to a heated tubular reactor with inert gas passing through it; after achieving a given temp. inert gas flow replaced by flow of Cl2 and SO2 (1:1); linear gas speed was 0.02-0.05 m/s; temp. was 550-750°C; volatiles trapped in cooled traps; monitored by X-ray diffraction and chem. analysis;
参考文献
Derlyukova; Vinokurova; Anufrieva
Russian Journal of Inorganic Chemistry, 2008 , vol. 53, # 9 p. 1371 - 1375
thionyl chloride in neat (no solvent) byproducts: SO2; reaction between 150 and 200 °C;;
参考文献
North, H. B.; Hageman, A. M.
Journal of the American Chemical Society, 1913 , vol. 35, p. 355 - 355
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Gmelin Handbook: Bi: MVol., 38, page 111 - 113
