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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氰芪
合成路线
（共 50 条）
292638-84-7
+
623-03-0
对氯苯甲腈
→
反应条件
13041-79-7
4-氰芪
反应条件
tetra-n-butylammonium acetate; palladium diacetate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine in 1,4-dioxane T=80°C; Heck reaction; 24 h; Inert atmosphereSealed tube;
参考文献
Xu, Hua-Jian; Zhao, Yong-Qiang; Zhou, Xin-Feng
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 8036 - 8041
108-86-1
溴代苯
+
3435-51-6
4-氰基苯乙烯
→
反应条件
13041-79-7
4-氰芪
反应条件
C32H44N4O8P2Pd; potassium carbonate in N,N-dimethyl-formamide T=60°C; Heck Reaction; 12 h; Inert atmosphereSchlenk technique;
参考文献
Shaikh, Tanveer Mahamadali; Hong, Fung-E
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1578 - 1588
292638-84-7
→
反应条件
13041-79-7
4-氰芪
反应条件
sodium acetate; [(t-butylselanyl-benzene)(PdOAc)]2 in N,N-dimethyl acetamide T=140°C; Heck reaction; 20 h;
参考文献
Organic Letters, , vol. 6, # 17 p. 2997 - 2999
292638-84-7
+
32792-60-2
→
反应条件
13041-79-7
4-氰芪
+
81329-28-4
反应条件
isoquinoline; lithium chloride; palladium dichloride in various solvent(s) T=160°C;
参考文献
Goossen, Lukas J.; Paetzold
Angewandte Chemie - International Edition, 2002 , vol. 41, # 7 p. 1237 - 1241
292638-84-7
+
3058-39-7
4-碘氰基苯
→
反应条件
13041-79-7
4-氰芪
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Heck reaction; 8 h;
参考文献
Li, Pinhua; Wang, Lei; Zhang, Lei; Wang, Guan-Wu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 7 p. 1307 - 1318
29822-79-5
→
反应条件
13041-79-7
4-氰芪
反应条件
C41H38BFeN3P2; hydrogen in tetrahydrofuran T=20 - 90°C; P=7500.75 Torr; 72 h; Inert atmosphere;
参考文献
Srimani, Dipankar; Diskin-Posner, Yael; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2013 , vol. 52, # 52 p. 14131 - 14134
Angew. Chem., 2013 , vol. 125, # 52 p. 14381 - 14383
100-52-7
苯甲醛
→
反应条件
13041-79-7
4-氰芪
+
1552-58-5
反应条件
1: p-cyanobenzaldehyde tosylhydrazone With potassium tert-butylate in toluene T=0 - 20°C; 1 h; 2: benzaldehyde With 5,10,15,20-tetraphenyl porphyrinato iron hydroxide; Aliquatreg; 336; phosphorous acid trimethyl ester in toluene T=40°C; Wittig olefination; 48 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 20 p. 6034 - 6035
→
反应条件
13041-79-7
4-氰芪
反应条件
2C8H8NO2(1-)*2Cl(1-)*2Pd(2+); tetrabutylammomium bromide; potassium carbonate in water T=120°C; Suzuki-Miyaura coupling; 14 h; Sealed vessel; stereoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 6 p. 2321 - 2327
292638-84-7
+
6068-72-0
对氰基苯甲酰氯
→
反应条件
13041-79-7
4-氰芪
反应条件
[{RhCl(C2H4)2}2] in o-xylene Mizoroki-Heck reaction; 6 h; Heating;
参考文献
Sugihara, Toru; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1765 - 1772
623-03-0
对氯苯甲腈
+
201852-49-5
→
反应条件
13041-79-7
4-氰芪
反应条件
C18H16Cl2O4Pd2; caesium carbonate; (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl in N,N-dimethyl-formamide T=120°C; 20 h; Inert atmosphere;
参考文献
Alacid, Emilio; Najera, Carmen
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8191 - 8195
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