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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
130447-21-1
合成路线
（共 12 条）
1041479-71-3
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
51554-93-9
1-(4-溴苯基)辛烷
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-72-4
+
130447-21-1
→
反应条件
1205517-14-1
+
92-86-4
4,4-二溴联苯
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
1041479-70-2
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
14310-24-8
4-溴联苄基
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
→
反应条件
92-86-4
4,4-二溴联苯
+
14310-24-8
4-溴联苄基
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
6731-23-3
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
2051-99-2
1-溴-4-异丁基苯
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
反应条件
palladium diacetate; 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran; hexane T=10°C; Inert atmosphere;
参考文献
Li, Jing; Jin, Liqun; Liu, Chao; Lei, Aiwen
Chemical Communications, 2013 , vol. 49, # 83 p. 9615 - 9617
130447-21-1
→
反应条件
106-40-1
对溴苯胺
反应条件
1: With acetone O-(2,4,6-trimethylphenylsulfonyl)oxime in tetrahydrofuran T=20°C; Amination; 3 h; 2: With hydrogenchloride; water T=20°C; Hydrolysis; 2 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 21 p. 3139 - 3142
6731-23-3
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
2051-99-2
1-溴-4-异丁基苯
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
→
反应条件
57774-35-3
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 1.) 20 deg C, 12 h, 2.) 60 deg C, 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 390, # 3 p. 389 - 398
1041479-70-2
+
130447-21-1
→
反应条件
92-86-4
4,4-二溴联苯
+
14310-24-8
4-溴联苄基
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
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