2,2-二甲基戊二酸二甲酯合成路线 （共 13 条）
反应条件
sulfuric acid T=50°C; 24 h;
参考文献
Hutchinson; Riendeau; Brideau; Chan; Delorme; Denis; Falgueyret; Fortin; Guay; Hamel; Jones; Macdonald; McFarlane; Piechuta; Scheigetz; Tagari; Therien; Girard
Journal of Medicinal Chemistry, 1993 , vol. 36, # 19 p. 2771 - 2787
反应条件
sulfuric acid 48 h; Heating;
参考文献
McCaffrey, Vanessa P.; Harbron, Elizabeth J.; Forbes, Malcolm D. E.
Macromolecules, 2005 , vol. 38, # 8 p. 3342 - 3350
反应条件
potassium carbonate in water T=20°C; 18 h;
参考文献
Mogi, Muneto; Yamada, Ken; Yasoshima, Kayo; Kawanami, Toshio; Umemura, Ichiro; Iwaki, Yuki; Qin, Hongbo; Imase, Hidetomo
Patent: US2009/118287 A1, 2009 ;
Location in patent: Page/Page column 72 ;
反应条件
in dichloromethane; hexafluoroisopropyl alcohol T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Ratnikov, Maxim O.; Tumanov, Vasily V.; Smit, William A.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 50 p. 9739 - 9742
反应条件
1: KI / ethanol; H2O 2: aq. HCl 3: aq. H2SO4 / CH2Cl2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 27, p. 1288 - 1294
反应条件
1: aq. HCl 2: aq. H2SO4 / CH2Cl2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 27, p. 1288 - 1294
反应条件
1.) CCl4, 3 h, 20 deg C; Yield given. Multistep reaction;
参考文献
Rousseau, Gerard; Blanco, Luis
Tetrahedron Letters, 1985 , vol. 26, # 35 p. 4191 - 4194
参考文献
Gazzetta Chimica Italiana, , vol. 109, p. 95 - 97
反应条件
di-tert-butyl peroxide T=150°C; 0.5 h; other ester; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 6 p. 948 - 952
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1327 - 1333
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Brown,R.F.; Schmid,G.H.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1288 - 1294
