1-(3-苯基)-3,3-二乙基三氮烯合成路线 （共 8 条）
反应条件
sodium carbonate in water T=5 - 10°C; 0.5 h;
参考文献
Ludwig, Miroslav; Valaskova, Pavla; Pytela, Oldrich
Collection of Czechoslovak Chemical Communications, 1994 , vol. 59, # 2 p. 401 - 411
反应条件
hydrogenchloride; potassium carbonate; sodium nitrite 1) H2O, 0 degC, 30 min; Multistep reaction;
参考文献
Ku, Hao; Barrio, Jorge R.
Journal of Organic Chemistry, 1981 , vol. 46, p. 5239 - 5241
反应条件
sulfonic acid resin (H+ form); lithium bromide 0.5 h; Heatingvar. of time, var. solvents, var. nucleophiles, var. triazenes; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 55, # 15 p. 4560 - 4564
反应条件
chloro-trimethyl-silane; lithium bromide in acetonitrile T=60°C; 0.333333 h;
参考文献
Ku, Hao; Barrio, Jorge R.
Journal of Organic Chemistry, 1981 , vol. 46, p. 5239 - 5241
反应条件
hydrogen bromide 0.5 h; Heating; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 55, # 15 p. 4560 - 4564
反应条件
sulfonic acid resin (H+ form); lithium bromide 0.5 h; Heatingvar. of time, var. solvents, var. nucleophiles, var. triazenes; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 55, # 15 p. 4560 - 4564
参考文献
Picherit; Wagner; Uguen
Tetrahedron Letters, 2004 , vol. 45, # 12 p. 2579 - 2583
反应条件
azodiisobutyric acid dinitrile in further solvent(s)
byproducts: C6H6, (C2H5)2NH, C2H6; reaction for 6 h at 80°C in cumol in presence of azoisobutyric acid dinitrile;;
参考文献
Hollaender, J.; Neumann, W. P.
Angewandte Chemie, 1971 , vol. 83, p. 850 - 851
Full Text Show Details
Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2.4.2, page 22 - 31
