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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
130562-15-1
合成路线
（共 5 条）
130562-15-1
→
反应条件
2627-86-3
(S)-(-)- α-甲基苄胺
反应条件
1: H2 / Raney-nickel W2 / ethanol / 24 h / 3750.3 Torr / Ambient temperature 2: HCO2NH4 / 10percent Pd/C / methanol / 0.5 h / Heating View Scheme
参考文献
Bringmann, G.; Geisler, J.-P.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 1 p. 67 - 73
130562-15-1
→
反应条件
21003-56-5
+
130562-16-2
反应条件
hydrogen in isopropanol acetate T=35°C; P=15001.5 Torr; 24 h; optical yield given as percent dediastereoselective reaction;
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
130562-15-1
→
反应条件
21003-56-5
+
130562-16-2
反应条件
hydrogen in isopropanol acetate T=35°C; P=15001.5 Torr; 24 h; optical yield given as percent dediastereoselective reaction;
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
130562-15-1
→
反应条件
68285-25-6
反应条件
1: H2 / Raney-nickel W2 / ethanol / 24 h / 3750.3 Torr / Ambient temperature 2: 79 percent / HCO2NH4 / 10percent Pd/C / methanol / 0.5 h / Heating View Scheme
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
130562-15-1
→
反应条件
21003-56-5
+
130562-16-2
反应条件
hydrogen in isopropanol acetate T=35°C; P=15001.5 Torr; 24 h; optical yield given as percent dediastereoselective reaction;
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
