4-(4-硝基苯)哌嗪-1-羧酸叔丁酯合成路线 (共 7 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 19 p. 5592 - 5599
反应条件
1: in dichloromethane T=20°C; 1.5 h; 2: With sodium tris(acetoxy)borohydride in dichloromethane T=20°C; 3 h; 3: With sodium hydroxide; water in dichloromethane
参考文献
US2007/167435 A1, ;
Page/Page column 47 ;
US 20070167435 A1
反应条件
triethylamine in dichloromethane
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Archiv der Pharmazie, , vol. 333, # 8 p. 267 - 274
反应条件
1: ethanol / 1 h / Heating 2: Et3N / CH2Cl2 / 20 °C View Scheme
参考文献
Archiv der Pharmazie, , vol. 333, # 8 p. 267 - 274
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 3 h;
参考文献
Palimkar, Sanjay S.; More, Vijaykumar S.; Kumar, P. Harish; Srinivasan, Kumar V.
Tetrahedron, 2007 , vol. 63, # 51 p. 12786 - 12790
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 2 h;
参考文献
Wang, Yuqiang
Patent: US2004/34033 A1, 2004 ;
Location in patent: Page/Page column 12; Sheet 1 ;