2,5-二碘-1,4-苯二醇合成路线 （共 24 条）
反应条件
boron tribromide in dichloromethane T=-78 - 20°C; 5 h;
参考文献
UNIVERSITA' DEGLI STUDI DI BARI; CONSIGLIO NAZIONALE DELLE RICERCHE; UNIVERSITA'DEGLI STUDI DEL SALENTO
Patent: WO2008/96239 A1, 2008 ;
Location in patent: Page/Page column 29 ;
反应条件
boron tribromide in dichloromethane T=20°C; Inert atmosphereCooling with acetone-dry ice;
参考文献
Pasquini, Chiara; Coniglio, Alessandra; Bassetti, Mauro
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6191 - 6194,4
反应条件
hydrogenchloride; methanol 4 h; Heating;
参考文献
Chai, Wen-Yu; Shi, Zi-Fa; An, Peng; Wang, Wei; Wang, Lu-Feng; Cao, Xiao-Ping
Chemistry - An Asian Journal, 2012 , vol. 7, # 1 p. 143 - 155
反应条件
1: 80 percent / I2; Hg(OAc)2 / CH2Cl2 / 25 °C 2: 95 percent / aq. HCl; methanol / 4 h / Heating View Scheme
参考文献
Chai, Wen-Yu; Shi, Zi-Fa; An, Peng; Wang, Wei; Wang, Lu-Feng; Cao, Xiao-Ping
Chemistry - An Asian Journal, 2012 , vol. 7, # 1 p. 143 - 155
反应条件
1: 75 percent / K2CO3 / acetone / 12 h / Heating 2: 80 percent / I2; Hg(OAc)2 / CH2Cl2 / 25 °C 3: 95 percent / aq. HCl; methanol / 4 h / Heating View Scheme
参考文献
Shi, Zi-Fa; Wang, Le-Jia; Wang, Hong; Cao, Xiao-Ping; Zhang, Hao-Li
Organic Letters, 2007 , vol. 9, # 4 p. 595 - 598
反应条件
1: iodine, HgO / ultrasound, 10 min, 90 deg C, 30 min 2: BBr3 / CH2Cl2 / 15 h / Ambient temperature View Scheme
参考文献
Huenig, Siegfried; Bau, Robert; Kemmer, Martina; Meixner, Hubert; Metzenthin, Tobias; et al.
European Journal of Organic Chemistry, 1998 , # 2 p. 335 - 348
反应条件
1: sulfuric acid; iodine; periodic acid / dichloromethane; water; acetic acid / 15 h / 75 °C 2: boron tribromide / dichloromethane / 20 °C / Inert atmosphere; Cooling with acetone-dry ice View Scheme
参考文献
Li, Jie; Meng, Jie; Huang, Xiaobo; Cheng, Yixiang; Zhu, Chengjian
Polymer, 2010 , vol. 51, # 15 p. 3425 - 3430
参考文献
Tan, Chunyan; Pinto, Mauricio R; Schanze, Kirk S
Chemical communications (Cambridge, England), 2002 , # 5 p. 446 - 447
反应条件
potassium hydroxide in dimethyl sulfoxide T=20°C;
参考文献
Liu, Yao; Jiang, Shujun; Schanze, Kirk S.
Chemical Communications, 2003 , # 5 p. 650 - 651
反应条件
potassium hydroxide in dimethyl sulfoxide; acetone 24 h; RefluxInert atmosphereSchlenk technique;
参考文献
Pasquini, Chiara; Coniglio, Alessandra; Bassetti, Mauro
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6191 - 6194,4
