2,5-二碘-1,4-苯二醇合成路线 (共 24 条)
反应条件
sodium hydroxide in water
4 h; Inert atmosphereReflux;
参考文献
Zhao, Xiaoyong; Schanze, Kirk S.
Chemical Communications, 2010 , vol. 46, # 33 p. 6075 - 6077
反应条件
1: K2CO3 / butan-2-one / Heating
2: NaOH / methanol / Heating
View Scheme
参考文献
Kuroda, Kenichi; Swager, Timothy M.
Chemical Communications, 2003 , # 1 p. 26 - 27
反应条件
1: 70 percent / K2CO3; KI / butan-2-one / 72 h / Heating
2: 76 percent / Pd(PPh3)4; CuI; DIPA / toluene / 24 h / 80 °C
3: 80 percent / KOH / methanol; tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Breen, Craig A.; Deng, Tao; Breiner, Thomas; Thomas, Edwin L.; Swager, Timothy M.
Journal of the American Chemical Society, 2003 , vol. 125, # 33 p. 9942 - 9943
反应条件
potassium carbonate in butanone
24 h; Heating;
参考文献
Kim, Ik-Bum; Dunkhorst, Anna; Gilbert, James; Bunz, Uwe H.F.
Macromolecules, 2005 , vol. 38, # 11 p. 4560 - 4562