lithium T=-196°C; P=0.005 Torr; Mechanism;

暂无反应条件数据

1) -130 deg C, 2) 0 deg C, ether; Yield given. Multistep reaction;

in diethyl ether; pentane addn. of soln. of Me3SnCl to soln. of Li-compound (prepd. in situ) at -120°C, warming to room temp.; shaking with water, drying and concn. of org. phase; anal. and GC;