(R)-(+)-1-苄基丙三醇合成路线 （共 40 条）
反应条件
potassium hydroxide in toluene Heating;
参考文献
Schott, Herbert; Schwendener, Reto A.
Liebigs Annales, 1996 , # 3 p. 365 - 369
反应条件
pyridine in dichloromethane T=-78 - 0°C;
参考文献
Matsumoto, Kazutsugu; Fuwa, Seiji; Shimojo, Megumi; Kitajima, Hidehiko
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 10 p. 2977 - 2987
反应条件
sodium methylate T=135°C; 2 h;
参考文献
LaMontagne, Maurice P.; Smith, David C.; Wu, Geng-Shuen
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 295 - 299
反应条件
phthalimide-containing resin; triphenylphosphine; hydrazine; diethylazodicarboxylate 1) THF, RT, 2 h, 2) EtOH, CH2Cl2, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Aronov, Alex M.; Gelb, Michael H.
Tetrahedron Letters, 1998 , vol. 39, # 28 p. 4947 - 4950
反应条件
sodium hydride in N,N-dimethyl-formamide 6 h; Ambient temperature;
参考文献
Fronza, Giovanni; Fuganti, Claudio; Mele, Andrea; Pedrocchi-Fantoni, Giuseppe; Sarra, Antonella; Servi, Stefano
Gazzetta Chimica Italiana, 1995 , vol. 125, # 7 p. 305 - 308
反应条件
1: 100 percent / thionyl chloride / CH2Cl2 / 0.5 h / -78 °C 2: 82 percent / dimethylformamide / Ambient temperature View Scheme
参考文献
Takano, Seiichi; Akiyama, Masashi; Sato, Seiji; Ogasawara, Kunio
Chemistry Letters, 1983 , p. 1593 - 1596
反应条件
di(n-butyl)tin oxide; cesium fluoride 1) toluene, 1 h, reflux, 2) DMF, r.t., 10 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nagashima; Ohno
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 8 p. 1972 - 1982
反应条件
sodium periodate in water T=20 - 25°C; 23 h;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: WO2006/132390 A1, 2006 ;
Location in patent: Page/Page column 29-30 ;
反应条件
1: NaIO4 View Scheme
参考文献
Wang; Chen; Liu; Wong
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1917 - 1920
反应条件
(i) TsCl, Py, (ii) NaOMe, MeOH; Multistep reaction;
参考文献
Anisuzzaman,A.K.M.; Owen,L.N.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 1021 - 1026
