tri-iso-propylsilane; trifluoroacetic acid in dichloromethane 4 h;
参考文献
Chou, Stanley S.; De, Mrinmoy; Kim, Jaemyung; Byun, Segi; Dykstra, Conner; Yu, Jin; Huang, Jiaxing; Dravid, Vinayak P.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4584 - 4587
hydrogenchloride in methanol 4 h; Heating; Yield given;
参考文献
Choi, Inseong; Kim, Young-Kwan; Min, Dal-Hee; Lee, Sangwook; Yeo, Woon-Seok
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16718 - 16721
1: 63 percent / 50percent aq. sodium hydroxide / 24 h / 100 °C 2: AIBN / methanol / 6 h / Irradiation 3: 0.1 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Choi, Inseong; Kim, Young-Kwan; Min, Dal-Hee; Lee, Sangwook; Yeo, Woon-Seok
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16718 - 16721
1: 63 percent / 50percent aq. sodium hydroxide / 24 h / 100 °C 2: AIBN / methanol / 6 h / Irradiation 3: 0.1 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Pale-Grosdemange, Catherine; Simon, Ethan S.; Prime, Kevin L.; Whitesides, George M.
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 12 - 20
1: AIBN / methanol / 6 h / Irradiation 2: 0.1 M HCl / methanol / 4 h / Heating View Scheme
参考文献
Pale-Grosdemange, Catherine; Simon, Ethan S.; Prime, Kevin L.; Whitesides, George M.
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 12 - 20
Choi, Inseong; Kim, Young-Kwan; Min, Dal-Hee; Lee, Sangwook; Yeo, Woon-Seok
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16718 - 16721
1: sodium hydroxide / ethanol; benzene; water / 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C / |Inert atmosphere 3: sodium hydroxide / water / 1 h / 90 °C 4: trifluoroacetic acid; tri-iso-propylsilane / dichloromethane / 4 h View Scheme
参考文献
Chou, Stanley S.; De, Mrinmoy; Kim, Jaemyung; Byun, Segi; Dykstra, Conner; Yu, Jin; Huang, Jiaxing; Dravid, Vinayak P.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4584 - 4587
1: triethylamine / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: sodium hydroxide / water / 1 h / 90 °C 3: trifluoroacetic acid; tri-iso-propylsilane / dichloromethane / 4 h View Scheme
参考文献
Chou, Stanley S.; De, Mrinmoy; Kim, Jaemyung; Byun, Segi; Dykstra, Conner; Yu, Jin; Huang, Jiaxing; Dravid, Vinayak P.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4584 - 4587