硫代乙酸 S-(29-羟基-12,15,18,21,24,27-六氧杂二十九烷-1-基)酯合成路线 (共 4 条)
反应条件
2,2'-azo-bisisobutyronitrile in tetrahydrofuran T=20°C; 3 h; Inert atmosphereUV-irradiation;
参考文献
Chemistry - A European Journal, , vol. 16, # 23 p. 7017 - 7029
反应条件
1: 65 percent / aq. NaOH / 24 h / 100 °C 2: 98 percent / AIBN / tetrahydrofuran / 12 h / Heating View Scheme
参考文献
Chemistry - A European Journal, , vol. 9, # 9 p. 1909 - 1921
反应条件
1: 65 percent / aq. NaOH / 24 h / 100 °C 2: 98 percent / AIBN / tetrahydrofuran / 12 h / Heating View Scheme
参考文献
Chemistry - A European Journal, , vol. 9, # 9 p. 1909 - 1921
反应条件
hydrogenchloride in methanol 4 h; Heating; Yield given;
参考文献
Pale-Grosdemange, Catherine; Simon, Ethan S.; Prime, Kevin L.; Whitesides, George M.
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 12 - 20