(3R,6R)-3,6-二甲基-1,4-二恶烷-2,5-二酮合成路线 （共 30 条）
反应条件
hydrogen in methanol T=125°C; P=112511 Torr; 12 h; Autoclave; Overall yield = 90 percentChromat.; stereoselective reaction;
参考文献
Shuklov, Ivan A.; Dubrovina, Natalia V.; Schulze, Joachim; Tietz, Wolfgang; Kuehlein, Klaus; Boerner, Armin
Chemistry - A European Journal, 2014 , vol. 20, # 4 p. 957 - 960
反应条件
[RuH(CO)(BPy-tPNN*)]; hydrogen in tetrahydrofuran T=110°C; P=38002.6 Torr; 12 h; Inert atmosphere;
参考文献
Balaraman, Ekambaram; Fogler, Eran; Milstein, David
Chemical Communications, 2012 , vol. 48, # 8 p. 1111 - 1113
反应条件
hydrogen in methanol T=125°C; P=112511 Torr; 12 h; Autoclave; Overall yield = 90 percentChromat.; stereoselective reaction;
参考文献
Shuklov, Ivan A.; Dubrovina, Natalia V.; Schulze, Joachim; Tietz, Wolfgang; Kuehlein, Klaus; Boerner, Armin
Chemistry - A European Journal, 2014 , vol. 20, # 4 p. 957 - 960
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=20°C; 48 h;
参考文献
Shuklov, Ivan A.; Jiao, Haijun; Schulze, Joachim; Tietz, Wolfgang; Kuehlein, Klaus; Boerner, Armin
Tetrahedron Letters, 2011 , vol. 52, # 9 p. 1027 - 1030
反应条件
Ca[N(SiMe3)2]2*2THF in toluene T=30°C; 0.166667 h;
参考文献
Phomphrai, Khamphee; Pracha, Supathana; Phonjanthuek, Phenphak; Pohmakotr, Manat
Dalton Transactions, 2008 , # 23 p. 3048 - 3050
反应条件
hydrogen in methanol T=150°C; P=112511 Torr; 15 h; Autoclave; Reagent/catalyst; chemoselective reaction;
参考文献
Shuklov, Ivan A.; Dubrovina, Natalia V.; Schulze, Joachim; Tietz, Wolfgang; Kuehlein, Klaus; Boerner, Armin
Chemistry - A European Journal, 2014 , vol. 20, # 4 p. 957 - 960
反应条件
1: polylactic acid 0.333333 h; 2: L-lactide T=200°C; 0.0833333 - 7.5 h;
参考文献
CARGILL, INCORPORATED
Patent: EP1247808 A2, 2002 ;
Location in patent: Page 15 ;
反应条件
water T=60 - 80°C; Hydrolysis; Kinetics; Further Variations:SolventsTemperaturesReagents;
参考文献
Conn
Food and Chemical Toxicology, 1995 , vol. 33, # 4 p. 273 - 283
反应条件
Ca[N(SiMe3)2]2*2THF in toluene T=30°C; 1 h;
参考文献
Phomphrai, Khamphee; Pracha, Supathana; Phonjanthuek, Phenphak; Pohmakotr, Manat
Dalton Transactions, 2008 , # 23 p. 3048 - 3050
反应条件
Ca[N(SiMe3)2]2*2THF in toluene T=30°C; 0.0833333 h;
参考文献
Phomphrai, Khamphee; Pracha, Supathana; Phonjanthuek, Phenphak; Pohmakotr, Manat
Dalton Transactions, 2008 , # 23 p. 3048 - 3050
