4-硝基苯基-2-乙酰氨基-3,4,6-O-三乙酰基-2-脱氧-β-D-吡喃葡萄糖苷合成路线 （共 15 条）
反应条件
sodium methylate in methanol
参考文献
Roy, Rene; Tropper, Francois D.; Morrison, Tara; Boratynski, Janusz
Journal of the Chemical Society, Chemical Communications, 1991 , # 7 p. 536 - 538
反应条件
1: methanol; sodium methylate / 20 °C 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / N,N-dimethyl-formamide / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
1: 97 percent / NaOCH3; MeOH / CHCl3 2: 4-TsOH*H2O / dimethylformamide / 20 °C 3: pyridine / 1.5 h / 0 °C 4: 6.19 g / AcOH; H2O / 3 h / 70 °C 5: 86 percent / pyridine / CH2Cl2 / 20 °C View Scheme
参考文献
Chen, Hong-Ming; Withers, Stephen G.
Carbohydrate Research, 2007 , vol. 342, # 15 p. 2212 - 2222
反应条件
1: 91.3 percent / H2 / 10percent Pd/C / ethanol; dioxane / 3 h / 760 Torr / Ambient temperature 2: 61.8 percent / 28percent NaOMe / methanol; acetonitrile; CHCl3 / 1 h / Ambient temperature View Scheme
参考文献
Roy, Rene; Tropper, Francois D.; Morrison, Tara; Boratynski, Janusz
Journal of the Chemical Society, Chemical Communications, 1991 , # 7 p. 536 - 538
反应条件
sodium acetate in acetonitrile
T=25°C; pH=5; 168 h; Product distribution; Further Variations:Reagents;
参考文献
Mendes, Adriano A.; Rodrigues, Dasciana S.; Filice, Marco; Fernandez-Lafuente, Roberto; Guisan, Jose M.; Palomo, Jose M.
Tetrahedron, 2008 , vol. 64, # 47 p. 10721 - 10727
