potassium carbonate in N,N-dimethyl-formamide T=40°C; 3 h;

1: 89 percent / pyridine / 20 °C 2: potassium carbonate / acetone / Heating View Scheme

potassium carbonate in acetone Methylation; Heating;

diethyl ether; acetone

1.1: potassium carbonate; water / methanol / 1 h / 20 °C 2.1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 110 °C 3.1: N-bromosuccinmide / N,N-dimethyl-formamide / 16 h / 20 °C 4.1: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethylene glycol dimethyl ether; water / 12 h / 60 °C / |Inert atmosphere 5.1: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C 5.2: 16 h / 20 °C 6.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 48 h / 20 °C 7.1: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 5 h / 0 - 45 °C 7.2: 0 - 20 °C 8.1: palladium 10 on activated carbon; hydrogen / methanol / 6 h / 22502.3 Torr View Scheme

potassium carbonate in methanol; water 0.333333 h; Ambient temperature;

1: LiAlH4 2: H2 / Pd-C 3: K2CO3 View Scheme

1: 97.4 g / sodium methoxide / methanol / 3 h / 20 °C 2: 81 percent / potassium carbonate / butan-2-one / 2.5 h / Heating View Scheme

1: LiAlH4 2: K2CO3 View Scheme

methanol; sodium hydroxide T=40°C;