6-(乙硫基)-2,2'-联吡啶合成路线 （共 13 条）
反应条件
1: monoperhydroxyphthalic acid magnesium salt / methanol / Ambient temperature 2: 1) n-BuLi / 1) Et2O or THF, -78 deg C 2) THF, -78 deg C View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 32 p. 4625 - 4628
反应条件
1: Mg-monoperoxyphthalate / methanol / 1 h / Ambient temperature
2: 1) n-BuLi / 1) Et2O, hexane, THF, -78 deg C, 2) THF, -78 deg C, 5 min
3: 1) n-BuLi / 1) Et2O-hexane-THF, -78 deg C, 5-10 min, 2) -78 deg C
View Scheme
参考文献
Uenishi, Jun'ichi; Tanaka, Takakazu; Nishiwaki, Kenji; Wakabayashi, Shoji; Oae, Shigeru; Tsukube, Hiroshi
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4382 - 4388
反应条件
1: Mg-monoperoxyphthalate / methanol / 1 h / Ambient temperature
2: 1) n-BuLi / 1) Et2O, hexane, THF, -78 deg C, 2) THF, -78 deg C, 5 min
View Scheme
参考文献
Uenishi, Jun'ichi; Tanaka, Takakazu; Nishiwaki, Kenji; Wakabayashi, Shoji; Oae, Shigeru; Tsukube, Hiroshi
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4382 - 4388
