反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '4123663', constants.ctx, '0')">diisobutylaluminium hydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=-78°C; 5 h; Inert atmosphere; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '2037554', constants.ctx, '0')">sulfuric acid</a>; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=-78 - 20°C; 20 h; <br />
参考文献
Lindsay, Vincent N. G.; Nicolas, Cyril; Charette, Andre B. Journal of the American Chemical Society, 2011 , vol. 133, # 23 p. 8972 - 8981
