反应条件
1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
2: water; mercury dichloride; mercury(II) oxide / acetonitrile / 3 h / 70 °C
3: methanol; sodium tetrahydroborate / 1 h / 0 - 5 °C
4: triethylamine / dichloromethane / 0 - 20 °C
5: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 10 h / 20 °C
View Scheme
参考文献
Balasubramaniam, Sivaraman; Kommidi, Harikrishna; Aidhen, Indrapal Singh
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2683 - 2686