[{(η5-C5Me5)IrCl}2(μ-Cl)2]; caesium carbonate; p-benozquinone in 1,4-dioxane T=110°C; 20 h; Sealed tube;

<b>Multi-step reaction with 2 steps<br /> </b>1: 1.) LiAlH₄, 2.) EtOAc, H₂O / 1a.) THF, 0-5 deg C, 1b.) RT, 1h, 2.) 0-5 deg C, 30 min<br />2: tetrahydrofuran / 0.33 h / 0 - 5 &deg;C<br /> <br /> &nbsp;