(S)-4,5-异亚丙基-1-溴戊烷合成路线 (共 5 条)
参考文献
Ni, Chiyou; Matile, Stefan
Chemical Communications, 1998 , # 7 p. 755 - 756
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane 0.333333 h; Ambient temperature1.) 0 deg C; Yield given;
参考文献
Leggeri; Azzolina; Pirillo; Traverso
Farmaco, 1989 , vol. 44, # 3 p. 303 - 313
反应条件
1: LiAlH4 / diethyl ether / 1 h / Heating 2: CBr4, triphenylphosphine / CH2Cl2 / 0.33 h / Ambient temperature; 1.) 0 deg C View Scheme
参考文献
Leggeri; Azzolina; Pirillo; Traverso
Farmaco, 1989 , vol. 44, # 3 p. 303 - 313
反应条件
1: p-toluenesulphonic acid / 4 h / Heating 2: LiAlH4 / diethyl ether / 1 h / Heating 3: CBr4, triphenylphosphine / CH2Cl2 / 0.33 h / Ambient temperature; 1.) 0 deg C View Scheme
参考文献
Leggeri; Azzolina; Pirillo; Traverso
Farmaco, 1989 , vol. 44, # 3 p. 303 - 313
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
5 h; Yield given;
参考文献
Leggeri; Azzolina; Pirillo; Traverso
Farmaco, 1989 , vol. 44, # 3 p. 303 - 313