反应条件
1: 1.) O3, 2.) zinc dust, acetic acid / 1.) CH2Cl2, -30 deg C, 10min, 2.) H2O, -30 deg C, 0.5 h; warm to 20 deg C 2: 72 percent / trimethylsilyl triflate / CH2Cl2 / 1.) -78 deg C, 0.5 h, 2.) -35 - -30 deg C, 5 h 3: 7 percent / 10percent palladised charcoal / ethyl acetate / 168 h / 20 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2441 - 2452
