1-羟基-1,2-苯碘酰-3(1H)-酮合成路线 （共 44 条）
反应条件
1: With palladium diacetate in N,N-dimethyl-formamide T=60°C; Addition; 3 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; Hydrolysis;
参考文献
Xia, Min; Chen, Zhenchu
Synthetic Communications, 2000 , vol. 30, # 1 p. 63 - 68
反应条件
1: With palladium diacetate in N,N-dimethyl-formamide T=60°C; Addition; 3 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; Hydrolysis;
参考文献
Xia, Min; Chen, Zhenchu
Synthetic Communications, 2000 , vol. 30, # 1 p. 63 - 68
反应条件
acetic acid 0.166667 h;
参考文献
Yusubov, Mekhman S.; Wirth, Thomas
Organic Letters, 2005 , vol. 7, # 3 p. 519 - 521
反应条件
in acetonitrile Ambient temperature;
参考文献
Zhdankin, Viktor V.; Kuehl, Chris J.; Krasutsky, Alexei P.; Bolz, Jason T.; Mismash, Brian; et al.
Tetrahedron Letters, 1995 , vol. 36, # 44 p. 7975 - 7978
反应条件
sodium periodate; acetic acid in water
4 h; Reflux;
参考文献
Nicolai, Stefano; Waser, Jerome
Organic Letters, 2011 , vol. 13, # 23 p. 6324 - 6327
反应条件
in dichloromethane
T=0 - 20°C;
参考文献
Zhdankin, Viktor V.; Maydanovych, Olena; Herschbach, Jon; McDonald, Robert; Tykwinski, Rik R.
Journal of the American Chemical Society, 2002 , vol. 124, # 39 p. 11614 - 11615
反应条件
water-d2 in acetonitrile
T=50°C; 5.5 h;
参考文献
Ochiai, Masahito; Nakanishi, Akinobu; Ito, Takao
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4253 - 4259
反应条件
1: 2-iodo benzoic acid With sodium periodate; acetic acid in water
4 h; Reflux;
2: water T=20°C; 1 h;
参考文献
Huang, Hanchu; Zhang, Guojin; Gong, Li; Zhang, Shuaiyan; Chen, Yiyun
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2280 - 2283
反应条件
1: dimethylsulfoxide-d6
2: H2O / dimethylsulfoxide-d6
View Scheme
参考文献
Moss, Robert A.; Zhang, Hongmei
Journal of the American Chemical Society, 1994 , vol. 116, # 10 p. 4471 - 4472
反应条件
water in dimethylsulfoxide-d6
参考文献
Moss, Robert A.; Zhang, Hongmei
Journal of the American Chemical Society, 1994 , vol. 116, # 10 p. 4471 - 4472
