反应条件
in water pptn. of hydrous Zr-oxide by addn. of a 4M LiOH-soln. to soln. of the Zr-compound (pH 10.3-10.6) until a final pH of 13.5-14.0 is obtained; filtration, washing with H2O to a pH of 7, drying in air at 100°C, calcination at 500°C for 5h;; X-ray diffraction, X-ray photoelectron spectroscopy;;
参考文献
Sugiyama, S.; Shimodan, K.; Hayashi, H.; Shigemoto, N.; Miyaura, K.; et al.
Journal of Catalysis, 1993 , vol. 141, p. 279 - 286
