sulfuric acid in sulfuric acid Electrolysis; electrochemical conversion of LiCO3 into LiOH in aq. H2SO4 at temp. 30-40°C in membrane electrolyzer is suggested; soln. of LiOH cooled, evapd. and LiOH*H2O crystd.; product washed with LiOH soln. and dried; elem. anal.;
参考文献
Russian Journal of Applied Chemistry, , vol. 77, # 7 p. 1108 - 1116
in hexane 1.6 M n-BuLi in hexane, 48 h; ppt. was washed thoroughly with hexane and EtOH, dried in vac., elem. anal., detected by X-ray powder diffractometry;
参考文献
Journal of Physical Chemistry B, , vol. 106, # 16 p. 4053 - 4060
in neat (no solvent) LiOH*H2O and Ni acetate separately dissolved in H2O; mixed; pH adjusted to 8.5-9.5; heated at 110°C until they were dry; calcined at 300-500°C; monitored by X-ray diffraction;
in neat (no solvent) LiOH*H2O and Ni acetate separately dissolved in H2O; mixed; pH adjusted to 8.5-9.5; heated at 110°C until they were dry; calcined at 600°C; monitored by X-ray diffraction;
in melt La-, Al-salts mixed with NaOH, LiOH*H2O milled for 30 min, dried for 1 hat 120°C, fired at 250 and 350°C in air for 3 h at 5.degr ee.C/min, cooled to room temp.; suspended in H2O, filtered, dried at 120°C for 3 h; monitored by XRD;
参考文献
Mendoza-Mendoza, Esmeralda; Montemayor, Sagrario M.; Escalante-Garcia, Jose I.; Fuentes, Antonio F.
Journal of the American Ceramic Society, 2012 , vol. 95, # 4 p. 1276 - 1283
in gaseous matrix Irradiation (UV/VIS); heating of powd. LiOH monohydrate in tantalum boat at 820 K, entraining of resulting LiOH vapour in a flow of N2 into central chamber, pulsed photolysis of LiOH vapour; detection by laser induced fluorescence spectroscopy;
参考文献
Plane, John M. C.; Rajasekhar, B.
Journal of the Chemical Society, Faraday Transactions 2: Molecular and Chemical Physics, 1988 , vol. 84, p. 273 - 286
