Lever, F. M.; Powell, A. R.
J. Chem. Soc. (London) A, 1969 , p. 1477 - 1482
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Lever, F. M.; Powell, A. R.
Intern. Conf. Coord. Chem., London 1959, Lectures Abstr., S. 135/136
Harris, G. S.
Journal of the Chemical Society, 1958 , p. 512 - 519
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Gmelin Handbook: P: MVol.C, 273, page 626 - 629
in neat (no solvent)
N2-atmosphere; condensation of HBr at -196°C onto V-complex (54percent purity; prepd. from VCl3(THF)3, Na and phosphine ligand by pptn. with pentane and drying), slow warming to room temp. with stirring, evapn., drying (high vac.), addn. of aq. NaOH;
参考文献
Gailus, Hartmut; Woitha, Claus; Rehder, Dieter
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 23 p. 3471 - 3478
byproducts: H2O; with dilute aq. sodium hydroxide;
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Glemser; v. Halasz
Inorganic and Nuclear Chemistry Letters, 1968 , vol. 4, p. 191,192, 193
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Glemser, O.; Halasz, S. P. von
Zeitschrift fuer Naturforschung, 1968 , vol. 23b, p. 743 - 745
