二(2-甲氧基苯基)甲酮合成路线 （共 39 条）
反应条件
1: methoxybenzene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane T=-55 - 20°C; Metallation; 3 h; 2: N,N-dimethylcarbamoyl chloride in diethyl ether; hexane T=-50 - 0°C; Acylation; 3 h;
参考文献
Verkerk, Udo; Fujita, Megumi; Dzwiniel, Trevor L.; McDonald, Robert; Stryker, Jeffrey M.
Journal of the American Chemical Society, 2002 , vol. 124, # 34 p. 9988 - 9989
反应条件
bis(1,5-cyclooctadiene)nickel (0) in N,N-dimethyl-formamide T=50°C; 3 h;
参考文献
Goto, Toshio; Onaka, Makoto; Mukaiyama, Teruaki
Chemistry Letters, 1980 , p. 51 - 52
反应条件
9,10-anthracenedicarbonitrile; oxygen in acetonitrile Irradiationinvestigation of the electron-transfer photooxygenation in the presence of 9,10-dicyanoanthracene; MechanismProduct distributionQuantum yield;
参考文献
Gollnick, Klaus; Schnatterer, Albert; Utschick, Gerald
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6049 - 6056
参考文献
Morton; Brachman
Journal of the American Chemical Society, 1954 , vol. 76, p. 2980,2983
反应条件
NiBr2bipy; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide Ambient temperatureelectrolysis;
参考文献
Dolhem; Ocafrain; Nedelec; Troupel
Tetrahedron, 1997 , vol. 53, # 50 p. 17089 - 17096
反应条件
N,N,N',N,-tetramethylethylenediamine; α-n-hexadecene; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; Suzuki reaction; P=3750.38 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Neumann, Helfried; Brennfuehrer, Anne; Beller, Matthias
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3645 - 3652
反应条件
lt;2,2',3,3',5,5'-hexaphenyl-(1,1'-biphenyl)-4,4'-dioxylgt;; oxygen; copper(l) chloride in various solvent(s) T=95°C; 25.7333 h; Yield given;
参考文献
Barbiero; Kim; Hay
Tetrahedron Letters, 1994 , vol. 35, # 32 p. 5833 - 5836
反应条件
tris-(dibenzylideneacetone)dipalladium(0); di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in N,N-dimethyl-formamide T=100°C; Inert atmosphere;
参考文献
Tolnai, Gergely L.; Petho, Balint; Krall, Peter; Novaka, Zoltan
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 125 - 129
反应条件
diethyl ether; lithium und Behandeln des erhaltenen Reaktionsgemisches mit festem CO2;
参考文献
Dolhem; Ocafrain; Nedelec; Troupel
Tetrahedron, 1997 , vol. 53, # 50 p. 17089 - 17096
反应条件
n-butyllithium; diethyl ether und Behandeln des erhaltenen Reaktionsgemisches mit festem CO2;
参考文献
Gilman; Bebb
Journal of the American Chemical Society, 1939 , vol. 61, p. 109 Anm.4
Journal of the American Chemical Society, 1940 , vol. 62, p. 987
