4'-(4-甲氧基苯基)-2,2':6',2''-三吡啶合成路线 （共 6 条）
反应条件
ammonium acetate 0.1 h; microwave irradiation;
参考文献
Tu, Shujiang; Li, Tuanjie; Shi, Feng; Wang, Qian; Zhang, Jinpeng; Xu, Jianing; Zhu, Xiaotong; Zhang, Xiaojing; Zhu, Songlei; Shi, Daqing
Synthesis, 2005 , # 18 art. no. F08805SS, p. 3045 - 3050
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C 2: aq. NH3 / various solvent(s) / 2 h / 100 °C View Scheme
参考文献
Synthesis, , # 17 p. 2873 - 2878
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C 2: aq. NH3 / various solvent(s) / 2 h / 100 °C View Scheme
参考文献
Synthesis, , # 17 p. 2873 - 2878
反应条件
ammonium acetate; sodium hydroxide 1.) 180 deg C, 2 h, 2.) 120 deg C, 2 h;
参考文献
Spahni, Werner; Calzaferri, Gion
Helvetica Chimica Acta, 1984 , vol. 67, # 54 p. 450 - 454
反应条件
acetic acid Heating;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 7, p. 1275 - 1282
反应条件
sodium hydroxide; hydrogen bromide
1.) acetic acid, 130 deg C, 3 h, 2.) CH2Cl2;
参考文献
Spahni, Werner; Calzaferri, Gion
Helvetica Chimica Acta, 1984 , vol. 67, # 54 p. 450 - 454
