苯并(3,4)-6-氧杂雌甾-1,3,5(10),8-四烯-17beta-醇合成路线 （共 6 条）
反应条件
hydrogen; palladium on activated charcoal
参考文献
Ramesh Babu; Ramana; Ramadas
Steroids, 1990 , vol. 55, # 3 p. 101 - 104
反应条件
1: 60 percent / 40percent methanol. Triton-B, t-butanol / xylene / 6 h / Heating 2: 60 percent / p-toluenesulfonic acid / benzene / 10 h / Ambient temperature 3: 95 percent / NaBH4 / methanol; tetrahydrofuran / 2 h / Ambient temperature 4: 60 percent / H2 / 10percent Pd/C View Scheme
参考文献
Ramesh Babu; Ramana; Ramadas
Steroids, 1990 , vol. 55, # 3 p. 101 - 104
反应条件
1: 95 percent / tetrahydrofuran / 1.) -20 deg C, 2.) reflux, 12 h 2: 60 percent / 40percent methanol. Triton-B, t-butanol / xylene / 6 h / Heating 3: 60 percent / p-toluenesulfonic acid / benzene / 10 h / Ambient temperature 4: 95 percent / NaBH4 / methanol; tetrahydrofuran / 2 h / Ambient temperature 5: 60 percent / H2 / 10percent Pd/C View Scheme
参考文献
Ramesh Babu; Ramana; Ramadas
Steroids, 1990 , vol. 55, # 3 p. 101 - 104
反应条件
1: 60 percent / 40percent methanol. Triton-B, t-butanol / xylene / 6 h / Heating 2: 60 percent / p-toluenesulfonic acid / benzene / 10 h / Ambient temperature 3: 95 percent / NaBH4 / methanol; tetrahydrofuran / 2 h / Ambient temperature 4: 60 percent / H2 / 10percent Pd/C View Scheme
参考文献
Ramesh Babu; Ramana; Ramadas
Steroids, 1990 , vol. 55, # 3 p. 101 - 104
反应条件
1: 95 percent / NaBH4 / methanol; tetrahydrofuran / 2 h / Ambient temperature 2: 60 percent / H2 / 10percent Pd/C View Scheme
参考文献
Ramesh Babu; Ramana; Ramadas
Steroids, 1990 , vol. 55, # 3 p. 101 - 104
反应条件
1: 60 percent / p-toluenesulfonic acid / benzene / 10 h / Ambient temperature 2: 95 percent / NaBH4 / methanol; tetrahydrofuran / 2 h / Ambient temperature 3: 60 percent / H2 / 10percent Pd/C View Scheme
参考文献
Ramesh Babu; Ramana; Ramadas
Steroids, 1990 , vol. 55, # 3 p. 101 - 104
