4-氰基-2’-甲氧基苯甲酮合成路线 (共 3 条)
反应条件
3,4,7,8-tetra-methyl-1,10-phenanthroline; oxygen; caesium carbonate; cobalt(II) chloride in toluene; acetonitrile T=80°C; 12 h;
参考文献
Karthikeyan, Jaganathan; Parthasarathy, Kanniyappan; Cheng, Chien-Hong
Chemical Communications, 2011 , vol. 47, # 37 p. 10461 - 10463
反应条件
N,N,N',N,-tetramethylethylenediamine; α-n-hexadecene; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; Suzuki reaction; P=3750.38 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 14, # 12 p. 3645 - 3652
反应条件
1: 2-methoxybromobenzene With magnesium in tetrahydrofuran Heating; 2: [4-cyanophenyl]methanone in tetrahydrofuran T=0 - 20°C; 3 h; 3: With dipyridinium dichromate; 4 A molecular sieve in dichloromethane T=20°C; 2 h; Further stages.;
参考文献
Tetrahedron, , vol. 64, # 11 p. 2586 - 2595