N-Boc-2-哌啶乙酸甲酯合成路线 （共 24 条）
反应条件
1: 2.15 g / thionyl chloride / 3 h / Heating 2: 48 percent / triethylamine; 4-(dimethylamino)pyridine / CHCl3 / 24 h 3: Burkholderia cepacia PS-C II lipase / diisopropyl ether; butan-1-ol / 168 h / 47 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 18, # 2 p. 181 - 191
反应条件
1: 48 percent / triethylamine; 4-(dimethylamino)pyridine / CHCl3 / 24 h 2: Burkholderia cepacia PS-C II lipase / diisopropyl ether; butan-1-ol / 168 h / 47 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 18, # 2 p. 181 - 191
反应条件
1: Jones reagent 2: 80 percent / 4-dimethylaminopyridine, 1,3-dicyclocyclohexylcarbodiimide / diethyl ether / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 20 p. 2903 - 2908
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; Reduction; 0.5 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 17 p. 2621 - 2624
