sodium amalgam

1: 37 percent / 6percent sodium amalgam, disodium hydrogenphosphate, sodium dihydrogenphosphate / tetrahydrofuran; methanol / -78 °C 2: trimethylamine / CHCl3 / 3.5 h / Heating 3: methanol / CH2Cl2 / 0.17 h / Heating View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587189', constants.ctx, '0')">hydrogen</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '11378922', constants.ctx, '0')">palladium on activated charcoal</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 67 percent / 26 h / 85 &deg;C<br />2: 99 percent / H₂ / 10percent Pd/C / acetonitrile<br /> <br /> &nbsp;

<b>Multi-step reaction with 4 steps<br /> </b>1: 97 percent / AlCl₃ / CH₂Cl₂ <br />2: 99 percent / NaF / methanol; H₂O / 0.25 h / 10 &deg;C<br />3: 81 percent / CH₂Cl₂ / 9000720 Torr<br />4: 99 percent / H₂ / Pd/C / methanol<br /> <br /> &nbsp;