N-苄氧羰基-L-苯丙氨酰基-L-苯丙氨酸合成路线 (共 27 条)
反应条件
triethylamine in water; acetonitrile T=20°C;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Synthesis, 2004 , # 16 p. 2645 - 2652
反应条件
anhydrous calcium nitrate; triethylamine in N,N-dimethyl-formamide T=20°C; Condensation; 2 h;
参考文献
Raydnov, M. G.; Klimenko, L. V.; Mitin, Yu. V.
Russian Journal of Bioorganic Chemistry, 1999 , vol. 25, # 5 p. 283 - 287
Bioorganicheskaya Khimiya, 1999 , vol. 25, # 5 p. 323 - 328
反应条件
1: N-benzyloxycarbonyl-L-phenylalanine With chloroformic acid ethyl ester; triethylamine in tetrahydrofuran T=0°C; 0.5 h; 2: L-phenylalanine in water T=0°C; 0.5 h;
参考文献
Verardo; Gorassini
Journal of Peptide Science, 2013 , vol. 19, # 5 p. 315 - 324
参考文献
Kanosue, Yoshifumi; Kojima, Satoshi; Hiraga, Yoshikazu; Ohkata, Katsuo
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 6 p. 1187 - 1193
反应条件
1: Et3N; DMAP / acetonitrile / 0.75 h / 20 °C 2: Et3N / acetonitrile; H2O / 1.67 h / 20 °C View Scheme
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Synthesis, 2004 , # 16 p. 2645 - 2652
反应条件
tetrabutylammomium bromide; sodium hydroxide in water T=0°C; 0.5 h; Reagent/catalystConcentration;
参考文献
Verardo; Gorassini
Journal of Peptide Science, 2013 , vol. 19, # 5 p. 315 - 324
反应条件
Tris buffer; triethylamine; α-chymotrypsin in acetonitrile T=30°C; Acylation; pH=7.8; 1 h;
参考文献
Miyazawa, Toshifumi; Ensatsu, Eiichi; Hiramatsu, Makoto; Yanagihara, Ryoji; Yamada, Takashi
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 396 - 401
反应条件
Tris buffer; triethylamine; α-chymotrypsin in acetonitrile T=30°C; Acylation; pH=7.8; 1 h;
参考文献
Miyazawa, Toshifumi; Ensatsu, Eiichi; Hiramatsu, Makoto; Yanagihara, Ryoji; Yamada, Takashi
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 396 - 401
反应条件
triethylamine in water; acetonitrile T=20°C; 1.66667 h;
参考文献
Gagnon, Paul; Huang, Xicai; Therrien, Eric; Keillor, Jeffrey W.
Tetrahedron Letters, 2002 , vol. 43, # 43 p. 7717 - 7719
反应条件
Carbonate buffer; potassium chloride; alpha-cyclodextrin in acetonitrile T=25°C; other cyclodextrins; Rate constant;
参考文献
Ueoka, Ryuichi; Matsumoto, Yoko; Harada, Katsuhiko; Akahoshi, Hirohiko; Ihara, Yasuji; Kato, Yasuo
Journal of the American Chemical Society, 1992 , vol. 114, # 21 p. 8339 - 8340