(1R,3R,4R,6S)-4,5,6-三(苯基甲氧基)环己烷-1,2,3-三醇合成路线 （共 14 条）
反应条件
hydrogenchloride in methanol 0.666667 h; Heating;
参考文献
Desai, Trupti; Fernandez-Mayoralas, Alfonso; Gigg, Jill; Gigg, Roy; Payne, Sheila
Carbohydrate Research, 1990 , vol. 205, # 1 p. 105 - 123
反应条件
1: sodium hydride / dimethylformamide 2: 91 percent / H2O, dichlorodicyanoquinone / CH2Cl2 / 0.75 h / 20 °C 3: 1.2 g / pyridine / 12 h / 20 °C 4: sodium hydroxide / methanol / 0.25 h / Heating 5: M HCl / methanol / 0.67 h / Heating View Scheme
参考文献
Desai, Trupti; Fernandez-Mayoralas, Alfonso; Gigg, Jill; Gigg, Roy; Payne, Sheila
Carbohydrate Research, 1990 , vol. 205, # 1 p. 105 - 123
反应条件
1: 1.2 g / pyridine / 12 h / 20 °C 2: sodium hydroxide / methanol / 0.25 h / Heating 3: M HCl / methanol / 0.67 h / Heating View Scheme
参考文献
Desai, Trupti; Fernandez-Mayoralas, Alfonso; Gigg, Jill; Gigg, Roy; Payne, Sheila
Carbohydrate Research, 1990 , vol. 205, # 1 p. 105 - 123
反应条件
hydrogen; palladium dihydroxide in methanol T=20°C; 24 h;
参考文献
Takahashi; Kittaka; Ikegami
Journal of Organic Chemistry, 2001 , vol. 66, # 8 p. 2705 - 2716
