(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran
T=20°C; 0.25 h;
参考文献
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Doklady Chemistry, 1993 , vol. 332, # 1-3 p. 195 - 197
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hydrogenchloride in toluene
byproducts: BrMgCl; n-heptylmagnesium bromide added dropwise at 0°C over 30 min to stoich. amt. of organotin chloride suspended in toluene under inert atm.; mixt. refluxed for 6 h; cooled to room temp.; hydrolyzed with 7percent HCl; org. layer sepd.; dried overnight (anhyd. Na2SO4); filtered; solvent evapd.; purified by vac. distn.; elem. anal.;
参考文献
Sadiq-ur-Rehman; Ali, Saqib; Badshah, Amin
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Uzbeksk. Khim. Zh., 1961 , p. 49 - 54
C. A., 1961 , p. 20922
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.15.1, page 353 - 359
