反应条件
1: 44 percent / Dibal / tetrahydrofuran; toluene / 0.5 h / 0 °C
2: 72 percent / Swern-oxid.
3: 78 percent / diethyl ether; tetrahydrofuran / 1) -10 deg C, 10 min., 2) 45 min.
4: 68 percent / PCC, AcONa / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Taber, Douglass F.; Hoerrner, R. Scott; Hagen, Michael D.
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1287 - 1289
