in neat (no solvent, solid phase) by a solid-state react. from the 4PbO2+PbO+MnO2+Sb2O3 mixt. in an evacuated sealed silica tube; annealing at 650°C for 50 h; subsequent annealing for 50 h after regrinding; detd. by powder XRD;
参考文献
Abakumov, Artem M.; Rozova, Marina G.; Chizhov, Pavel S.; Antipov, Evgeny V.; Hadermann, Joke; Van Tendeloo, Gustaaf
Journal of Solid State Chemistry, 2004 , vol. 177, # 8 p. 2855 - 2861
in neat (no solvent) byproducts: Cl2, H2O; heating of NaCl with HNO3 and MnO2 in argillaceous retorts;; leaching residue containing NaNO3 and Mn(NO3)2;;
参考文献
Bradburn
Journal of the Society of Chemical Industry, London, 1889 , vol. 8, p. 707 - 707
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Gmelin Handbook: Na: MVol., 43.4, page 175 - 177
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Thompson
Patent: EP6710 , 1889 ;
in neat (no solvent, solid phase) nitride : oxide ratio= 1:4; molding into tablets; heating in air at 850°C; decomposition, burning; X-ray powder diffraction;
参考文献
Journal of Applied Chemistry USSR (English Translation), , vol. 61, p. 1939 - 1942
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 61, p. 2139 - 2142
in neat (no solvent, solid phase) Irradiation (UV/VIS); laser ablation of La-Ca-Mn-O target (mixture of oxides, nominal composition La0.67Ca0.33MnO3, calcination at 800°C for 5 h); laser beam 532nm (Nd:YAG laser); quadrupole and TOF mass spectrometry;
参考文献
Chemical Physics Letters, , vol. 300, # 5-6 p. 739 - 744
in neat (no solvent) heating MnO2 (dried by slight warming in vac.) with F2-N2-gas-mixt. (vol.-ratio 20:80) to 150 °C;;
参考文献
Aynsley, E. E.; Peacock, R. D.; Robinson, P. L.
Journal of the Chemical Society, 1950 , p. 1622 - 1624
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Gmelin Handbook: Mn: MVol.C1, 2.6.8.3.4, page 300 - 301
