air in neat (no solvent, solid phase)
byproducts: CO, H2O; Fe-contg. compd. was mixed with Ni-contg. compd. at the molar ratio Fe:Ni=0.5; mixt. was ground and calcined at 400°C for 2.5 h in staticair; cooling to room temp.; the powder was dispersed in distd. water an d stirred at 80°C for 1 h; the compds. were recovered by filtration and dried under ambient conditions; detd. by powder XRD;
参考文献
Chen, Fengxi; Zhong, Ziyi; Xu, Xiao-Jun; Chen, Yuxiang
Journal of Solid State Chemistry, 2004 , vol. 177, # 11 p. 4368 - 4371
