in neat (no solvent)
byproducts: H2O; heated with a heating rate of 10°C/min under static air atm. to temp. above 420°C; monitored by X-ray diffraction;
参考文献
Czakis-Sulikowska; Radwanska-Doczekalska; Czylkowska; Markiewicz; Broniarczyk
Journal of Thermal Analysis and Calorimetry, 2006 , vol. 86, # 2 p. 327 - 335
in neat (no solvent)
byproducts: H2O; heated in air flow or in static air at a heating rate of 10 K/min in Pt crucibles up to 1273 K; verified by X-ray diffraction and IR spectroscopy;
参考文献
Ferenc; Cristovao; Sarzynski
Journal of Thermal Analysis and Calorimetry, 2006 , vol. 86, # 3 p. 783 - 789
in neat (no solvent)
byproducts: Cl2, CO2, H2O; also H2O as by-product; heated in N2 or air atm. at flow rate of 100 mL/min at heating rate of 5-40°C/min; monitored by IR-spectroscopy;
