反应条件
1.1: 100 percent / NaH / dimethylformamide / 6 h / 85 °C
2.1: 82 percent / 4 h / 240 °C
3.1: LiAlH4 / tetrahydrofuran / 12 h / Heating
3.2: 71 percent / aq. HCl / tetrahydrofuran
4.1: 91 percent / Et3N / petroleum ether / 48 h / 50 °C
5.1: 85 percent / trifluoroacetic acid / 2.5 h / 0 °C
View Scheme
参考文献
Nishide, Kiyoharu; Miyamoto, Tetsuo; Kumar, Kamal; Ohsugi, Shin-Ichi; Node, Manabu
Tetrahedron Letters, 2002 , vol. 43, # 47 p. 8569 - 8573
