反应条件
1.1: sodium tetrahydroborate; methanol / tetrahydrofuran / 4 h / 50 - 55 °C 2.1: triethylamine / 4-(N,N-dimethlyamino)pyridine / dichloromethane / 6 h / 25 - 30 °C 3.1: sodium hydroxide / dimethyl sulfoxide / 0.17 h / 20 - 25 °C 3.2: 2 h / 50 - 55 °C View Scheme
参考文献
IND-SWIFT LABORATORIES LIMITED; BHIRUD, Shekhar Bhaskar; JOHAR, Perminder Singh; SHARMA, Ekta; JAMSHAD, Danish; PRAJAPATY, Ramkaran
Patent: WO2011/92719 A2, 2011 ;
